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31.
冶金石灰是石灰石经过工业煅烧的产品。其二氧化碳含量低,且经过高温煅烧后基本不含有机物。无需按照《石灰石、白云石化学分析国家标准中二氧化碳的化学分析方法》中用酸进行试样分解,只需在1200℃高温中灼烧,使石灰中残留的或煅烧后吸收空气中二氧化碳而形成的碳酸盐分解,象通常测定含碳耐火材料中二氧化碳那样,采用气体容量法进行测定。 相似文献
32.
A novel series of temperature‐sensitive poly[(N‐isopropylacrylamide)‐co‐(ethyl methacrylate)] (p(NIPAM‐co‐EMA)) microgels was prepared by the surfactant‐free radical polymerization of N‐isopropylacrylamide (NIPAM) with ethyl methacrylate (EMA). The shape, size dispersity and volume‐phase transition behavior of the microgels were investigated by transmission electron microscopy (TEM), ultraviolet–visible (UV–Vis) spectroscopy, dynamic light scattering (DLS) and differential scanning calorimetry (DSC). The transmission electron micrographs and DLS results showed that microgels with narrow distributions were prepared. It was shown from UV–Vis, DLS and DSC measurements that the volume‐phase transition temperature (VPTT) of the p(NIPAM‐co‐EMA) microgels decreased with increasing incorporation of EMA, but the temperature‐sensitivity was impaired when more EMA was incorporated, causing the volume‐phase transition of the microgels to become more continuous. It is noteworthy that incorporation of moderate amounts of EMA could not only lower the VPTT but also enhance the temperature‐sensitivity of the microgels. The reason for this phenomenon could be attributed to changes in the complicated interactions between the various molecules. Copyright © 2004 Society of Chemical Industry 相似文献
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七号信令网管系统的数据库服务器采用惠普UNIX工作站及SYBASE数据库。由于采集的数据量增大,原先设计的数据库空间不能满足数据存储三个月的要求.因此采用一块外置硬盘对数据库空间进行扩展。详细地介绍了SYBASE数据库空间扩展的全过程。 相似文献
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F Javier Benítez Ana I Leal Francisco J Real Juan L Acero Gloria Roldán 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(3):309-316
BACKGROUND: The first stage of the cork industrial process generates great volumes of wastewater with moderate to high organic pollutant content that must be purified using different procedures, such as filtration by membranes. RESULTS: The tangential filtration of these wastewaters was studied using two different laboratory equipments. In the first one, three ultrafiltration (UF) membranes were tested, with molecular weight cut‐off (MWCO) 100 kDa and 30 kDa, and two operating modes were used: total recycling of permeate and retentate streams, and in continuous mode, without recycling both streams. In the total recycling UF experiments, the influence of the operating variables on the permeate flux was first established. The effectiveness of the different membranes was determined by evaluating the rejection coefficients for several parameters that measure the global pollutant content of the effluent. The values found for these rejection coefficients were in the following order: ellagic acid and color > absorbance at 254 nm > tannic content > COD (chemical oxygen demand). In the continuous mode experiments, the fouling mechanism for each membrane was established by fitting the experimental data to various filtration fouling models given in the literature. The operating mode in the second equipment was batch concentration, and additional experiments were carried out with an UF membrane (2 kDa), and with a NF membrane (with MWCO in the range 150–300 Da). CONCLUSIONS: The three operating modes tested provided different rejection levels of organic matter; among them, the most effective procedure tested was batch concentration mode using a NF membrane. Copyright © 2007 Society of Chemical Industry 相似文献
37.
L. M. CRUZ-ORIVE 《Journal of microscopy》2005,219(1):18-28
A new principle is presented to generate isotropic uniform random (IUR) test lines hitting a geometric structure in three-dimensional space (3D). The principle therefore concerns the estimation of surface area, volume, membrane thickness, etc., of arbitrary structures with piecewise smooth boundary. The principle states that a point-sampled test line on an isotropic plane through a fixed point in 3D is effectively an invariant test line in 3D. Particular attention is devoted to the stereology of particles, where an alternative to the surfactor method is obtained to estimate surface area. An interesting case arises when the particle is convex. The methods are illustrated with synthetic examples. 相似文献
38.
水库淤积初步平衡问题 总被引:2,自引:0,他引:2
水库淤积平衡问题对于确定淤积危害程度、可持续利用标准等都非常重要。本文通过分析大量已建、在建和规划水库淤积情况,对水库淤积初步平衡后淤积变化趋势与设计淤积标准等问题进行了讨论和商榷。研究表明,水库淤积初步平衡后,兴利库容淤积发展仍然很快,库尾河床与水位抬升仍在继续,并未最终稳定。水库淤积平衡应该更加注重兴利库容淤积情况和库尾河床与水位抬升趋势,仅仅关注总淤积量变化情况是不够的。从区域长远利益考虑,大江大河上的水库设计淤积年限还应大大加长。 相似文献
39.
常压渣油热反应过程中胶体的稳定性 总被引:10,自引:0,他引:10
利用质量分数电导率方法研究了中东和克拉玛依常压渣油在热反应过程中胶体的稳定性。结果表明,随着反应时间的增长,在热反应生焦诱导期内,渣油的胶体稳定性迅速下降;开始生焦后,胶体稳定性缓慢下降。从中东常压渣油的SARA四组分的数均相对分子质量、碳氢元素组成、平均芳碳率等方面探讨了中东常压渣油在热反应过程中胶体稳定性下降的原因。结果表明,在热反应中,由于裂解和缩聚反应的共同作用,使渣油的沥青质和饱和分含量上升,芳香分含量下降,胶质含量变化不大;随着热反应的进行,四组分的数均相对分子质量均呈下降趋势,导致了渣油胶体稳定性的下降并发生生焦反应。 相似文献
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